HPLC coupled with APCI (Atmospheric Pressure Chemical Ionisation)-MS seems to be the preferable technique for detection of sulphonamides. It was used to identify the sulphathiazole in edible trout tissue. A detection limit of 10 μg/kg and a quantitation limit of 30 μg/kg were obtained. MS data useful for the identification, confirmation and quantitation of sulphathiazole by APCI-MS have not been reported previously.
Identification of sulphathiazole by HPLC/APCI-MS in edible trout tissue / M. Bononi, E. de Dominicis, A. Fossati, F. Tateo. - In: ITALIAN JOURNAL OF FOOD SCIENCE. - ISSN 1120-1770. - 14:3(2002), pp. 295-299.
Identification of sulphathiazole by HPLC/APCI-MS in edible trout tissue
M. BononiPrimo
;F. TateoUltimo
2002
Abstract
HPLC coupled with APCI (Atmospheric Pressure Chemical Ionisation)-MS seems to be the preferable technique for detection of sulphonamides. It was used to identify the sulphathiazole in edible trout tissue. A detection limit of 10 μg/kg and a quantitation limit of 30 μg/kg were obtained. MS data useful for the identification, confirmation and quantitation of sulphathiazole by APCI-MS have not been reported previously.
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