A stereoselective synthesis of the C1–C9 fragment of (–)-dictyostatin has been achieved by use of a titanium(IV) chloride mediated chelation-controlled Mukaiyama aldol reaction and two modified Horner–Wadsworth–Emmons olefinations (Roush– Masamune and Still–Gennari).
A Practical Synthesis of the C1-C9 Fragment of Dictyostatin / C. Zanato, L.L. Pignataro, Z. Hao, C.M.A. Gennari. - In: SYNTHESIS. - ISSN 0039-7881. - 2008:14(2008), pp. C00408SS.2158-C00408SS.2162.
A Practical Synthesis of the C1-C9 Fragment of Dictyostatin
C. ZanatoPrimo
;L.L. PignataroSecondo
;C.M.A. GennariUltimo
2008
Abstract
A stereoselective synthesis of the C1–C9 fragment of (–)-dictyostatin has been achieved by use of a titanium(IV) chloride mediated chelation-controlled Mukaiyama aldol reaction and two modified Horner–Wadsworth–Emmons olefinations (Roush– Masamune and Still–Gennari).
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