The present work reports the synthesis and evaluation of antimicrobial activity of polyindole-TiO2 nanocomposite. Polyindole-TiO2 nanocomposite was synthesized by aqueous in situ chemical polymerization of indole using ammonium persulfate as an oxidant under ultrasonic condition. The synthesized polyindole and polyindole-TiO2 nanocomposites were characterized by ultraviolet-visible spectroscopy, Fourier transform infrared spectroscopy, scanning electron microscope, thermogravimetric analysis, and X-ray diffraction techniques. A sharp peak at approximate to 1,402cm(-1) is due to the stretching vibrations of OTiO bond in polyindole-TiO2 nanocomposite. The X-ray diffraction pattern shows the major diffraction peaks at 25 degrees C and 48 degrees C, indicating TiO2 in anatase form. Polyindole-TiO2 shows maximum activity against gram-positive Staphylococcus aureus and Bacillus subtilis as compared to gram-negative Escherichia coli
Ultrasound Synthesis of Polyindole-TiO2 Nanocomposite and Evaluation of Antibacterial Activity / H. Kalpana, W. Dipak, C. Prakash, C. Aniruddha, M. Kakasaheb, S. Dallavalle, B. Bahule, C. Vasant. - In: POLYMER-PLASTICS TECHNOLOGY AND ENGINEERING. - ISSN 0360-2559. - 56:12(2017), pp. 1259-1266. [10.1080/03602559.2016.1163581]
Ultrasound Synthesis of Polyindole-TiO2 Nanocomposite and Evaluation of Antibacterial Activity
S. Dallavalle;
2017
Abstract
The present work reports the synthesis and evaluation of antimicrobial activity of polyindole-TiO2 nanocomposite. Polyindole-TiO2 nanocomposite was synthesized by aqueous in situ chemical polymerization of indole using ammonium persulfate as an oxidant under ultrasonic condition. The synthesized polyindole and polyindole-TiO2 nanocomposites were characterized by ultraviolet-visible spectroscopy, Fourier transform infrared spectroscopy, scanning electron microscope, thermogravimetric analysis, and X-ray diffraction techniques. A sharp peak at approximate to 1,402cm(-1) is due to the stretching vibrations of OTiO bond in polyindole-TiO2 nanocomposite. The X-ray diffraction pattern shows the major diffraction peaks at 25 degrees C and 48 degrees C, indicating TiO2 in anatase form. Polyindole-TiO2 shows maximum activity against gram-positive Staphylococcus aureus and Bacillus subtilis as compared to gram-negative Escherichia coliFile | Dimensione | Formato | |
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