CHEMISTRY OF IRIDIUM CARBONYL CLUSTERS - SYNTHESIS AND CHEMICAL CHARACTERIZATION OF THE HEXANUCLEAR ANIONS [IR6(CO)15(CO2ME)]-, [IR6(CO)15(CO2ET)] AND [IR6(CO)14(CO2ME))2]2- - CRYSTAL AND MOLECULAR-STRUCTURE OF [N(PPH3)2][IR6(MU-CO)4(CO)11(CO2ME)]