Icosahedral carbonyl clusters [Ni10Sb2(μ 12-Ni)Ni(CO)32-(CO)18] n- (n = 2, 3 or 4); synthesis, spectroscopic, electrochemical and bonding analysis. Crystal structures of [Ni10Sb2(μ 12-Ni)Ni(CO)32(CO)18] n- (n = 2 or 3)