A new, high-yielding methodology for reducing hydrazones to hydrazines is described, which allows the synthesis of different mono-, di- and trisubstituted hydrazines. Moreover, the reduction step can be followed by an in situ reaction with a carboxylic acid making possible a 'one-pot' synthesis of trisubstituted hydrazides. The method is relatively general and, in principle, suitable for industrial applications.
A new 'one-pot' synthesis of hydrazides by reduction of hydrazones / D. Perdicchia, E. Licandro, M. Maiorana, C Baldoli, C. Giannini. - In: TETRAHEDRON. - ISSN 0040-4020. - 59:39(2003), pp. 7733-7742.
Titolo: | A new 'one-pot' synthesis of hydrazides by reduction of hydrazones |
Autori: | PERDICCHIA, DARIO (Primo) LICANDRO, EMANUELA (Secondo) GIANNINI, CLELIA (Ultimo) |
Parole Chiave: | Hydrazides; Hydrazines; Hydrazone reduction; Trimethylamine borane |
Settore Scientifico Disciplinare: | Settore CHIM/06 - Chimica Organica |
Data di pubblicazione: | 2003 |
Rivista: | |
Tipologia: | Article (author) |
Digital Object Identifier (DOI): | http://dx.doi.org/10.1016/S0040-4020(03)01208-0 |
Appare nelle tipologie: | 01 - Articolo su periodico |
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