A new, high-yielding methodology for reducing hydrazones to hydrazines is described, which allows the synthesis of different mono-, di- and trisubstituted hydrazines. Moreover, the reduction step can be followed by an in situ reaction with a carboxylic acid making possible a 'one-pot' synthesis of trisubstituted hydrazides. The method is relatively general and, in principle, suitable for industrial applications.
A new 'one-pot' synthesis of hydrazides by reduction of hydrazones / D. Perdicchia, E. Licandro, M. Maiorana, C Baldoli, C. Giannini. - In: TETRAHEDRON. - ISSN 0040-4020. - 59:39(2003), pp. 7733-7742.
A new 'one-pot' synthesis of hydrazides by reduction of hydrazones
D. PerdicchiaPrimo
;E. LicandroSecondo
;M. Maiorana;C. GianniniUltimo
2003
Abstract
A new, high-yielding methodology for reducing hydrazones to hydrazines is described, which allows the synthesis of different mono-, di- and trisubstituted hydrazines. Moreover, the reduction step can be followed by an in situ reaction with a carboxylic acid making possible a 'one-pot' synthesis of trisubstituted hydrazides. The method is relatively general and, in principle, suitable for industrial applications.
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