Resin-bound benzotriazole chemistry applied to the solid-phase synthesis of arrays of unsymmetrical aryl ureas is described here. The chemistry assessment process, the monomer rehearsal, the preparation of a discrete library by automated parallel synthesis, the parallel purification protocol employing solid-phase scavenging, and the complete analytical characterization of the library components are also presented.
Solid-Supported Benzotriazoles. 2. Synthetic Auxiliaries and Traceless Linkers for the Combinatorial Synthesis of Unsymmetrical Ureas / A. Paio, R.F. Crespo, P. Seneci, M. Ciraco. - In: JOURNAL OF COMBINATORIAL CHEMISTRY. - ISSN 1520-4766. - 3:4(2001), pp. 354-359.
Solid-Supported Benzotriazoles. 2. Synthetic Auxiliaries and Traceless Linkers for the Combinatorial Synthesis of Unsymmetrical Ureas
P. SeneciPenultimo
;
2001
Abstract
Resin-bound benzotriazole chemistry applied to the solid-phase synthesis of arrays of unsymmetrical aryl ureas is described here. The chemistry assessment process, the monomer rehearsal, the preparation of a discrete library by automated parallel synthesis, the parallel purification protocol employing solid-phase scavenging, and the complete analytical characterization of the library components are also presented.
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