1H and 13C NMR chemical shifts of α- and β-anomers of adenosine, 2'-deoxyadenosine and their acetate derivatives were completely and definitely assigned using the concerted application of one- and two-dimensional experiments (gCOSY, gNOESY, gHSQC, and gHMBC). The influence of the stereochemistry of the purine base on the NMR data of the hydrogen and carbon atoms of the furanose moiety was investigated.
Complete 1H and 13C NMR spectral assignment of of α- and β-adenosine, 2'-deoxyadenosine and their acetate derivatives / P. Ciuffreda, S. Casati, A. Manzocchi. - In: MAGNETIC RESONANCE IN CHEMISTRY. - ISSN 0749-1581. - 45:9(2007 Sep), pp. 781-784. [10.1002/mrc.2036]
Complete 1H and 13C NMR spectral assignment of of α- and β-adenosine, 2'-deoxyadenosine and their acetate derivatives
P. CiuffredaPrimo
;S. CasatiSecondo
;A. ManzocchiUltimo
2007
Abstract
1H and 13C NMR chemical shifts of α- and β-anomers of adenosine, 2'-deoxyadenosine and their acetate derivatives were completely and definitely assigned using the concerted application of one- and two-dimensional experiments (gCOSY, gNOESY, gHSQC, and gHMBC). The influence of the stereochemistry of the purine base on the NMR data of the hydrogen and carbon atoms of the furanose moiety was investigated.
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