A short parallel synthesis of b-D-galactopyranosyl-O-pyridinoline (Gal-PYD), a collagen glycoconjugated cross-link, and of Gal-epiPYD, a (5S)-epimer, useful as internal standard in the analytical evaluation of the natural isomer in human tissue, is reported.
Total synthesis of the collagen glycosylated cross-link β-d-galactopyranosyl-O-pyridinoline and of its unnatural epimer β-d-galactopyranosyl-O-epipyridinoline / P. Allevi, R. Colombo, E. Giannini, M. Anastasia. - In: TETRAHEDRON-ASYMMETRY. - ISSN 0957-4166. - 18:14(2007 Jul 30), pp. 1750-1757. [10.1016/j.tetasy.2007.07.006]
Total synthesis of the collagen glycosylated cross-link β-d-galactopyranosyl-O-pyridinoline and of its unnatural epimer β-d-galactopyranosyl-O-epipyridinoline
P. AlleviPrimo
;E. GianniniPenultimo
;M. AnastasiaUltimo
2007
Abstract
A short parallel synthesis of b-D-galactopyranosyl-O-pyridinoline (Gal-PYD), a collagen glycoconjugated cross-link, and of Gal-epiPYD, a (5S)-epimer, useful as internal standard in the analytical evaluation of the natural isomer in human tissue, is reported.
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