Cholesta-5,8-dien-3β-ol was synthesized in two steps by starting from 3β-acetoxycholesta-5,7-diene. Diethyl azodicarboxylate reacts with 3β-acetoxycholesta-5,7-diene to afford 3β-acetoxy-7α-(1,2-dicarbethoxyhydrazo)-cholesta-5,8-diene and 3β-acetoxy-7α-(1,2-dicarbethoxyhydrazo)cholesta-5,8(14)-diene. The former was then reduced with lithium in ethylamine to the title

Synthesis of cholesta-5,8-dien-3β-ol / M. Anastasia, A. Fiecchi, G. Galli. - In: JOURNAL OF ORGANIC CHEMISTRY. - ISSN 0022-3263. - 46:17(1981), pp. 3421-3422.

Synthesis of cholesta-5,8-dien-3β-ol

M. Anastasia
Primo
;
1981

Abstract

Cholesta-5,8-dien-3β-ol was synthesized in two steps by starting from 3β-acetoxycholesta-5,7-diene. Diethyl azodicarboxylate reacts with 3β-acetoxycholesta-5,7-diene to afford 3β-acetoxy-7α-(1,2-dicarbethoxyhydrazo)-cholesta-5,8-diene and 3β-acetoxy-7α-(1,2-dicarbethoxyhydrazo)cholesta-5,8(14)-diene. The former was then reduced with lithium in ethylamine to the title
cholesta 5,8 dien 3beta ol ; drug identification ; drug synthesis ; infrared spectrometry ; mass spectrometry ; proton nuclear magnetic resonance
Settore BIO/10 - Biochimica
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/2434/183901
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