The optical and radiochemical purification of the scintillating liquid which will fill the detector of the JUNO experiment plays a crucial role in achieving its scientific goals. Given its gigantic mass and dimensions, and an unprecedented target value of about 3 % at 1 MeV in energy resolution, JUNO has set severe requirements on the parameters of its scintillator, such as attenuation length (Lat > 20 m at 430 nm), light yield, and content of radioactive contaminants (238U, 232Th < 10-15 g/g). To accomplish these needs, the scintillator will be processed using several purification methods, including distillation under vacuum and gas stripping, carried out in two large-scale plants installed at the JUNO site. In this paper, the layout, operating principles, and technical aspects which have driven the design and construction of the distillation and gas stripping plants are reviewed. The distillation is effective in enhancing the optical properties and removing high-boiling radioactive impurities (238U, 232Th, 40K), while the stripping process exploits pure water steam and high-purity nitrogen to extract gaseous contaminants (222Rn, 39Ar, 85Kr, O2) from the scintillator. The plant operating parameters have been tuned during the recent commissioning phase at the JUNO site and several quality control measurements and tests have been performed to evaluate the performances of the plants. Preliminary results on the efficiency of these purification processes will be shown.

Distillation and gas stripping purification plants for the JUNO liquid scintillator / C. Landini, M. Beretta, P. Lombardi, A. Brigatti, M. Montuschi, S. Parmeggiano, E. Percalli, G. Ranucci, V. Antonelli, D. Basilico, B. Caccianiga, C. Coletta, M.G. Giammarchi, L. Miramonti, A.C. Re, P. Saggese, M.D.C. Torri, S. Aiello, G. Andronico, A. Barresi, A. Bergnoli, M. Borghesi, R. Brugnera, R. Bruno, A. Budano, A. Cammi, V. Cerrone, R. Caruso, D. Chiesa, C. Clementi, S. Dusini, A. Fabbri, G. Felici, A. Garfagnini, N. Giudice, A. Gavrikov, M. Grassi, R.M. Guizzetti, N. Guardone, B. Jelmini, L. Lastrucci, I. Lippi, L. Loi, C. Lombardo, F. Mantovani, S.M. Mari, A. Martini, M. Nastasi, D. Orestano, F. Ortica, A. Paoloni, F. Petrucci, E. Previtali, M. Redchuck, B. Ricci, A. Romani, G. Sava, A. Serafini, C. Sirignano, M. Sisti, L. Stanco, E.S. Farilla, V. Strati, A. Triossi, C. Tuve', C. Venettacci, G. Verde, L. Votano. - In: NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH. SECTION A, ACCELERATORS, SPECTROMETERS, DETECTORS AND ASSOCIATED EQUIPMENT. - ISSN 0168-9002. - 1069:(2024), pp. 169887.1-169887.11. [10.1016/j.nima.2024.169887]

Distillation and gas stripping purification plants for the JUNO liquid scintillator

M. Beretta
Secondo
;
E. Percalli;D. Basilico;M.G. Giammarchi;L. Miramonti;A.C. Re;M.D.C. Torri;
2024

Abstract

The optical and radiochemical purification of the scintillating liquid which will fill the detector of the JUNO experiment plays a crucial role in achieving its scientific goals. Given its gigantic mass and dimensions, and an unprecedented target value of about 3 % at 1 MeV in energy resolution, JUNO has set severe requirements on the parameters of its scintillator, such as attenuation length (Lat > 20 m at 430 nm), light yield, and content of radioactive contaminants (238U, 232Th < 10-15 g/g). To accomplish these needs, the scintillator will be processed using several purification methods, including distillation under vacuum and gas stripping, carried out in two large-scale plants installed at the JUNO site. In this paper, the layout, operating principles, and technical aspects which have driven the design and construction of the distillation and gas stripping plants are reviewed. The distillation is effective in enhancing the optical properties and removing high-boiling radioactive impurities (238U, 232Th, 40K), while the stripping process exploits pure water steam and high-purity nitrogen to extract gaseous contaminants (222Rn, 39Ar, 85Kr, O2) from the scintillator. The plant operating parameters have been tuned during the recent commissioning phase at the JUNO site and several quality control measurements and tests have been performed to evaluate the performances of the plants. Preliminary results on the efficiency of these purification processes will be shown.
Distillation; JUNO; LAB; Liquid scintillator; Purification; Stripping
Settore PHYS-01/A - Fisica sperimentale delle interazioni fondamentali e applicazioni
2024
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/2434/1105491
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