The synthesis of indolo-benzazepine, indolo-benzazocine and indolo-benzazonine derivatives using a palladium-catalyzed coupling reaction is described. The polycyclic systems were obtained in a few steps directly from commercially available materials. The coupling of substrates containing aryl bromides was improved by microwave irradiation.
Practical and efficient palladium-promoted synthesis of indole systems containing medium- and large-ring-fused heterocycles / E. Beccalli, G. Broggini, M. Martinelli, G. Paladino, E. Rossi. - In: SYNTHESIS. - ISSN 0039-7881. - 2006:14(2006), pp. 2404-2412.
Practical and efficient palladium-promoted synthesis of indole systems containing medium- and large-ring-fused heterocycles
E. BeccalliPrimo
;M. Martinelli;G. PaladinoPenultimo
;E. RossiUltimo
2006
Abstract
The synthesis of indolo-benzazepine, indolo-benzazocine and indolo-benzazonine derivatives using a palladium-catalyzed coupling reaction is described. The polycyclic systems were obtained in a few steps directly from commercially available materials. The coupling of substrates containing aryl bromides was improved by microwave irradiation.
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