The synthesis of the title compounds is presented. The functionalization of the C-19 carbon was carried out by photolysis of the appropriate 5α-bromo-6β-hydroxy analogs. Certain improvements of synthetic procedures are described in detail.
Preparation of 19 hydroxypregnenolone 3 acetate and 3 methyl ether / E. Santaniello, H.E.Hadd, E. Caspi. - In: JOURNAL OF STEROID BIOCHEMISTRY. - ISSN 0022-4731. - 6:11-12(1975), pp. 1505-1508.
Preparation of 19 hydroxypregnenolone 3 acetate and 3 methyl ether
E. SantanielloPrimo
;
1975
Abstract
The synthesis of the title compounds is presented. The functionalization of the C-19 carbon was carried out by photolysis of the appropriate 5α-bromo-6β-hydroxy analogs. Certain improvements of synthetic procedures are described in detail.
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