Reductive alkylation of ethylenediamine with benzaldehyde and hydrogen in the presence of Pd-C has been investigated in order to optimize the synthesis of N,N'-dibenzylethylenediamine; the efficiency of the procedure has been improved by minimizing undesired competing reactions of cyclization and hydrogenolysis.
Synthesis of N,N'-dibenzylethylenediamine via palladium-carbon-catalysed reductive alkylation / M. Pallavicini, E. Valoti, O. Piccolo. - In: JOURNAL OF CHEMICAL RESEARCH. SYNOPSES. - ISSN 0308-2342. - 1995:11(1995), pp. 472-473.
Synthesis of N,N'-dibenzylethylenediamine via palladium-carbon-catalysed reductive alkylation
M. PallaviciniPrimo
;E. ValotiSecondo
;
1995
Abstract
Reductive alkylation of ethylenediamine with benzaldehyde and hydrogen in the presence of Pd-C has been investigated in order to optimize the synthesis of N,N'-dibenzylethylenediamine; the efficiency of the procedure has been improved by minimizing undesired competing reactions of cyclization and hydrogenolysis.
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